Published April 1, 1974 | Version public
Journal Article

Nuclear magnetic resonance spectroscopy. Use of ¹³C spectra to establish configurations of oximes

Abstract

The use of ^(13)C nmr (cmr) spectra for the determination of configurations of oximes is described. The problems of quantitative analysis of syn-anti mixtures of oximes by cmr, because of differential T_1 and Overhauser effects, are considered. Chemical shifts for the cmr resonances of a number of aldehydes and ketones are reported.

Additional Information

© 1974 American Chemical Society. Received August 28, 1973. Supported by the Public Health Service, Research Grant No. GM-11072 from the Division of General Medical Sciences, and by the National Science Foundation.

Additional details

Additional titles

Alternative title
Nuclear magnetic resonance spectroscopy. Use of carbon-13 spectra to establish configurations of oximes
Alternative title
Use of ¹³C spectra to establish configurations of oximes
Alternative title
Use of carbon-13 spectra to establish configurations of oximes

Identifiers

Eprint ID
60932
DOI
10.1021/jo00922a001
Resolver ID
CaltechAUTHORS:20151008-153201653

Funding

U.S. Public Health Service (USPHS)
GM-11072
NSF

Dates

Created
2015-10-10
Created from EPrint's datestamp field
Updated
2023-09-27
Created from EPrint's last_modified field

Caltech Custom Metadata

Other Numbering System Name
Caltech Gates and Crellin Laboratories of Chemistry
Other Numbering System Identifier
4750