Published June 1, 1973 | Version public
Journal Article

Nuclear Magnetic Resonance Spectroscopy. Application of Pulse and Fourier Transform Carbon-13 Nuclear Magnetic Resonance Techniques to Structure Elucidation. Rauwolfia Alkaloids

Abstract

The natural-abundance pulse and Fourier transform ^(13)C nmr spectra of several Rauwolfia alkaloids have been recorded. Using noise-decoupling, partial single-frequency off-resonance deooupling (SFOR), and lanthanide chelate induced chemical-shift changes (lanthanide shifts), a self-consistent series of assignments have been made for the observed resonances.

Additional Information

© 1973 American Chemical Society. Received October 24, 1972. Supported by the Public Health Service, Research Grant No. GM-11072 from the Division of General Medical Sciences, and by the National Science Foundation. National Institutes of Health Postdoctoral Fellow, 1971-1972. NATO Postdoctoral Fellow, 1970-1971.

Additional details

Identifiers

Eprint ID
60944
Resolver ID
CaltechAUTHORS:20151009-133523120

Funding

U.S. Public Health Service (USPHS)
GM-11072
NSF
NIH Postdoctoral Fellowship
NATO Postdoctoral Fellowship

Dates

Created
2015-10-16
Created from EPrint's datestamp field
Updated
2021-11-10
Created from EPrint's last_modified field

Caltech Custom Metadata

Other Numbering System Name
Caltech Gates and Crellin Laboratories of Chemistry
Other Numbering System Identifier
4503